Browsing by Author "Becker, Thorsten"
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- ItemCreep damage assessment of ex-service 12% Cr power plant steel using digital image correlation and quantitative microstructural evaluation(MDPI, 2019) Van Rooyen, Melody; Becker, Thorsten; Westraadt, Johan; Marx, GeneveveENGLISH ABSTRACT: The lifetime of steam pipelines in long-term operation in coal-fired power plants are limited due to material damage that resulted from creep exposure. In the present study, the authors comparatively assess the damage of ex-service 12% Cr piping steel with varying degrees of exposure while using accelerated creep tests that employ digital image correlation (DIC) as well as microstructural investigation that is based on electron microscopy. The DIC technique, which allows multiple creep curves to be measured at temperatures ranging from 550–600 °C from a single specimen, revealed higher Zener–Hollomon parameters for a high damage material with a high void density when compared to a material with lower damage and lower void density. Both of the material states showed similar hardness values, subgrain sizes, and boundary character, despite the difference in void densities. Slightly higher inter-particle spacing of MX precipitates results in a lower threshold stress of 79 MPa for the high damage steel when compared to 97 MPa for the low damage material. Besides large Laves phase particles (>0.2 µm) that are found in the higher damaged materials that result in solid solution depletion, the most prominent microstructural damage indicator was a lower density of M₂₃C₆ precipitates. Therefore, the observations indicate that the Zener–Hollomon parameter and M₂₃C₆ particles are good damage assessment indicators between the most extreme damage states and they predict a lower damage level for a medium void density material.
- ItemHeat treatment of TI-6AL-4V produced by laserCUSING(SAIIE, 2015) Becker, Thorsten; Van Rooyen, Melody; Dimitrov, DimitriLaserCUSING® is a selective laser melting (SLM) process that is capable of manufacturing parts by melting powder with heat input from a laser beam. LaserCUSING demonstrates potential for producing the intricate geometries specifically required for biomedical implants and aerospace applications. One main limitation to this form of rapid prototyping is the lack of published studies on the material performance of the resulting material. Studies of the material’s performance are often complicated by dependence on several factors, including starting powder properties, laser parameters, and post-processing heat treatments. This study aims to investigate the mechanical properties of LaserCUSING-produced Ti-6Al-4V and its performance relative to the conventional wrought counterpart. A combination of conventional and LaserCUSING-tailored heat treatments is performed. The resulting microstructures are studied and linked to the properties obtained from hardness tests. The findings highlight that LaserCused Ti-6Al-4V is competitive with traditional materials, provided that optimal parameters are chosen and parts are subject to tailored post-processing. In the as-built condition, LaserCused Ti-6Al-4V displays superior strength and hardness as a result of a martensitic microstructure, and a poorer performance in ductility. However, the material performance can be improved using tailored heat treatments. Careful consideration must be given to suitable post-processing before application in critical components in the aerospace or biomedical industry can occur.
- ItemInfluence of heat treatments on the microstructure and tensile behaviour of selective laser melting-produced TI-6AL-4V parts(Southern African Institute for Industrial Engineering, 2016) Ter Haar, Gerrit Matthys; Becker, Thorsten; Blaine, Deborah C.ENGLISH ABSTRACT: In industry, post-process heat treatments of Ti-6Al-4V are performed with the aim of improving its tensile behaviour. While heat treatments of wrought Ti6Al4V have been standardised (e.g., Aerospace Material Specification H-81200), heat treatments of selective laser melting (SLM)-produced Ti-6Al-4V lacks research and understanding. Significant concern exists about SLM Ti6-Al-4V’s achievable ductility attributed to its martensitic (α’) phase. In this research, heat treatments at a range of temperatures are applied to SLM-produced Ti-6Al-4V tensile samples. Microstructural analysis (both optically and through electron backscatter diffraction) was used to identify links between heat treatments and microstructure. Subsequently, uniaxial tensile tests were performed to determine the respective tensile properties of all samples. Correlations in the data show a significant loss in strength with respect to an increase in annealing temperature due to grain growth, while no noticeable trend was observed for fracture strain with regard to annealing temperatures.